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Energy Catalyst International Incorporated
  • Home
  • Pipeline Maintenance
    • Summary
    • Product Presentation
  • Tank Maintenance
    • Summary
    • Application Notes
    • Lab Test Protocol
    • Product Calculator
    • Product Data Sheet
    • Recovery Procedure
    • SDS (Safety Data Sheet)
  • About
  • Contact

Recover - Lab Test Protocol

Test scenario

ECI used the following protocol to test the efficacy of Recover in a laboratory environment.


A sample of sludge was taken from a 350,000 BBL crude oil storage tank, with 12,000 BBLs of sludge in a firm (milkshake) consistency at the bottom of the tank.




Control sample

To the first beaker, a measured 200ml of the collected sludge, plus 400ml of crude oil from the same storage tank was added as diluting fluid.


This control sample was used to observe any solubilization (reduction) of the sludge just from contact with the crude

(without Recover).


 

Test sample

To the second, identical beaker, a measured 200ml of the collected sludge, plus 400ml of crude oil from the same storage tank was added as diluting fluid (same as the Control sample).


4ml of Recover was added to the Test sample.





Daily mixing for 4 days

Both the Control and Test samples were mixed twice daily for 30 seconds (once in the morning, once in the evening) over the first 4 days of the test.







Test results

Control sample

Control sample

Control sample

Day 1:

Sample created and stirred.

200ml of sludge at bottom of beaker.


Day 2:

Stirred twice.


Day 3:

Stirred twice.


Day 4:

Stirred twice.

200ml of sludge remains at bottom of beaker.

Test complete.




Conclusion:

Without Recover, the sludge is still very visible at bottom of beaker.



Sample of sludge is not refinable.

Test sample

Control sample

Control sample

Day 1:

Sample created & stirred.

200ml of sludge at bottom of beaker.


Day 2:

Stirred twice.


Day 3:

Stirred twice.

Even suspension from top to bottom of beaker.

Less than 1ml of material remaining at bottom of beaker.


Day 4:

Stirred twice.

No material remains at bottom of beaker.

Test complete.


Conclusion:

Recover has dissolved the sludge. Remaining volume of liquid in beaker consists of recovered crude oil and a small amount Recover.


Sample is refinable.

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